Static Headspace-Gas Chromatography Theory and Practice - livro usado

EAN (ISBN-13): 9780471749448
ISBN (ISBN-10): 0471749443
Livro de capa dura
Ano de publicação: 2006
Editor/Editora: Wiley-Interscience
349 Páginas
Peso: 0,635 kg
Língua: eng/Englisch

Livro na base de dados desde 2007-05-29T07:02:35-03:00 (Sao Paulo)
Página de detalhes modificada pela última vez em 2023-11-30T07:33:37-03:00 (Sao Paulo)
Número ISBN/EAN: 0471749443

Número ISBN - Ortografia alternativa:
0-471-74944-3, 978-0-471-74944-8
Ortografia alternativa e termos de pesquisa relacionados:
Autor do livro: kolb, bruno, ettre, leslie
Título do livro: rom, static, chromatography, sorry out gas, headspace, theory wants, the practice

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Dados da editora

Autor: Bruno Kolb; Leslie S. Ettre
Título: Static Headspace-Gas Chromatography - Theory and Practice
Editora: Wiley-Interscience; John Wiley & Sons
376 Páginas
Ano de publicação: 2006-06-13
Peso: 0,630 kg
Língua: Inglês
162,00 € (DE)
Not available (reason unspecified)
160mm x 238mm x 22mm

BB; Hardcover, Softcover / Chemie; Chromatographie; Chemie; Chemistry; Chromatographie / Trennverfahren; Chromatography / Separation Techniques; Gaschromatographie; Chromatographie / Trennverfahren

Preface. Preface to the First Edition. List of Acronyms and Symbols. 1. General introduction. 1.1 Principles of headspace analysis . 1.2 Types of headspace analysis. 1.3 The evolution of the HS-GC methods. 1.4 Headspace -- gas chromatography literature. 1.5 Regulatory methods utilizing (static) HS-GC. 1.6 References. 2. Theoretical background of HS-GC and its applications. 2.1 Basic theory of headspace analysis. 2.2 Basic physicochemical relationships. 2.3 Headspace sensitivity. 2.4 Headspace linearity. 2.5 Duplicate analyses. 2.6 Multiple headspace extraction (MHE). 2.7 References. 3. The technique of HS-GC. 3.1 Sample vials. 3.2 Caps. 3.3 Septa. 3.4 Thermostatting. 3.5 The fundamentals of headspace sampling systems. 3.6 Use of open-tubular (capillary) columns. 3.7 Enrichment techniques in HS-GC. 3.8 Special techniques with the balanced-pressure systems. 3.9. Reaction HS-GC. 3.10 References. 4. Sample handling in HS-GC. 4.1 Equilibration. 4.2 Solution approach. 4.3 Sample handling and sample introduction. 4.4 Preparation of standard solutions. 4.5 Influence of the matrix. 4.6 Methods aiming the complete evaporation of the analyte. 4.7 References. 5. Headspace methods for quantitative analysis. 5.1 Internal normalization. 5.2 Internal standard method. 5.3 External standard method. 5.4 Standard addition method. 5.5 Multiple headspace extraction (MHE). 5.6 Analysis of solid samples (adsorption systems). 5.7 Calibration techniques with headspace samples of varying volumes. 5.8 Analysis of gas samples. 5.9 References. 6. Method development in HS-GC. 6.1 General guidelines. 6.2 Determination of the residual monomer content of polystyrene pellets. 6.3 Determination of residual solvents in a printed plastic film. 6.4 Determination of the volatile constituents of a cathodic electrolytic plating bath. 7. Nonequilibrium static headspace analysis. 7.1 Accelerated analysis. 7.2 Heat-sensitive samples. 7.3 References. 8. Qualitative analysis by HS-GC. 8.1 The use of HS-GC in 'fingerprinting.'. 8.2 The use of headspace sampling in hyphenated systems. 8.3 The use of HS-GC in microbiology. 8.4 References. 9. Special measurements. 9.1 Determination of vapor pressures. 9.2 Determination of activity coefficients. 9.3 Determination of related physicochemical functions. 9.4 Determination of phase distribution (partition coefficient). 9.5 Reaction constant measurements. 9.6 Determination of solute solubility by MHE. 9.7 Gas-solid systems. 9.8 Validation of the headspace instrumentation: investigation of detector linearity and detection limit. 9.9 References. Index.